Navegação por autor "HWANG, JIANN-YANG"

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  • IPEN-DOC 22012

    KOMATSU, LUIZ G.H. ; PARRA, DUCLERC F. ; OLIANI, WASHINGTON L. ; LUGAO, ADEMAR B. ; RANGARI, VIJAYA K.. Degradation study of High Melt Sterngt Polypropylene/Clay nanocomposites in environmental and accelerated conditions. In: CARPENTER, JOHN S. (Ed.); BAI, CHENGUANG (Ed.); ESCOBEDO, JUAN P. (Ed.); HWANG, JIANN-YANG (Ed.); IKHMAYIES, SHADIA (Ed.); LI, BOWEN (Ed.); LI, JIAN (Ed.); MONTEIRO, SERGIO N. (Ed.); PENG, ZHIWEI (Ed.); ZHANG, MINGMING (Ed.) CHARACTERIZATION OF MINERALS, METALS, AND MATERIALS. 145th . ANNUAL MEETING & EXIBITION, February 14-18, 2016, Nashville, Tennessee, USA. Proceedings... New York: Wiley , 2016, 2016. p. 61-67. DOI: 10.1007/978-3-319-48254-5_8

    Palavras-Chave: decomposition; polypropylene; clays; nanocomposites; environment; aging; gamma radiation; thermal degradation

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  • IPEN-DOC 24663

    ARANTES, MARIANA M. ; SANTANA, JULYANA ; VALENZUELA-DIAZ, F.R.; RANGARI, VIJAY K.; GUVEN, OLGUN; MOURA, ESPERIDIANA A.B. . Development and characterization of recycled-HDPE/EVA foam reinforced with babassu coconut epicarp fiber residues. In: LI, BOWEN (Ed.); LI, JIAN (Ed.); IKHMAYIES, SHADIA (Ed.); ZHANG, MINGMING (Ed.); KALAY, YUNUS E. (Ed.); CARPENTER, JOHN S. (Ed.); HWANG, JIANN-YANG (Ed.); MONTEIRO, SERGIO N. (Ed.); FIRRAO, DONATO (Ed.); BROWN, ANDREW (Ed.); BAI, CHENGUANG (Ed.); PENG, ZHIWEI (Ed.); ESCOBEDO-DIAZ, JUAN P. (Ed.); GOSWAMI, RAMASIS (Ed.); KIM, JEONGGUK (Ed.). Characterization of Minerals, Metals, and Materials. TMS. Cham, CZ, Switzerland: Springer International Publishing AG, 2018. p. 497-506, (The Minerals, Metals & Materials Series). DOI: 10.1007/978-3-319-72484-3_52

    Abstract: Nowadays, the development of polymeric materials reinforced with residues of vegetal fibers is becoming popular for application in different segments, from the automotive to the civil construction and furniture industry. Vegetal fiber residues may be used as reinforcement of the recycled polymer materials, for instance, to produce foams to packaging or to thermal and acoustic isolation for green building application. This work is focused on the development and characterization of recycled-HDPE/EVA foam reinforced with fiber residues from babassu coconut epicarp. Firstly, composites based on recycled-HDPE/EVA blend reinforced with babassu coconut fiber were obtained by melting extrusion process. The composites were then extruded in a special single screw for foaming. The foam samples were submitted to mechanical tests, density measurement, DSC, TG, and FE-SEM analysis.

    Palavras-Chave: coconut palms; coconuts; fibers; polyethylenes; polymerization; polyvinyls; recycling

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  • IPEN-DOC 22470

    CARDOSO, ELIZABETH C.L. ; SEIXAS, MARCUS V.S.; WIEBECK, HELIO; OLIVEIRA, RENE R. ; MACHADO, GLAUSON A.F. ; MOURA, ESPERIDIANA A.B. . Development of bio-based foams prepared from PBAT/PLA reinforced with biio-calcium carbonate compatibilized by electron beam radiation. In: KHMAYIES, SHADIA (Ed.); LI, BOWEN (Ed.); CARPENTER, JOHN S. (Ed.); HWANG, JIANN-YANG (Ed.); MONTEIRO, SERGIO N. (Ed.); LI, JIAN (Ed.); FIRRAO, DONATO (Ed.); ZHANG, MINGMING (Ed.); PENG, ZHIWEI (Ed.); ESCOBEDO, JUAN P. (Ed.); BAI, CHENGUANG (Ed.) CHARACTERIZATION OF MINERALS, METALS, AND MATERIALS. 145th . ANNUAL MEETING & EXIBITION, February 14-18, 2016, Nashville, Tennessee, USA. Proceedings... New York: Wiley , 2016, 2016. p. 637-644. DOI: 10.1007/978-3-319-48210-1_80

    Palavras-Chave: electron beams; foams; calcium carbonates; eggs; wastes; composite materials; tensile properties; x-ray diffraction; ion microscopy; scanning electron microscopy; plastics; polymers; thermal gravimetric analysis

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  • IPEN-DOC 25625

    REIS, PEDRO R.S. ; SANTANA, JULYANA G. ; OLIVEIRA, RENE R. ; RANGARI, VIJAYA K.; LOURENÇO, FELIPE R.; MOURA, ESPERIDIANA A.B. . Development of biocomposite materials from biodegradable polymer and bio-hydroxyapatite derived from eggshells for biomedical applications. In: LI, BOWEN (Ed.); LI, JIAN (Ed.); IKHMAYIES, SHADIA (Ed.); ZHANG, MINGMING (Ed.); KALAY, YUNUS E. (Ed.); CARPENTER, JOHN S. (Ed.); HWANG, JIANN-YANG (Ed.); MONTEIRO, SERGIO N. (Ed.); BAI, CHENGUANG (Ed.); ESCOBEDO-DIAZ, JUAN P. (Ed.); SPENA, PASQUALE R. (Ed.); GOSWAMI, RAMASIS (Ed.). Characterization of Minerals, Metals, and Materials. Cham, CZ, Switzerland: Springer Nature Switzerland AG, 2019. p. 571-581, (The Minerals, Metals & Materials Series). DOI: 10.1007/978-3-030-05749-7_57

    Abstract: Nowadays, significant advances have been made in the development of biodegradable polymeric materials for biomedical applications. This study aims to prepare and characterize composite materials based on PLA/PBAT, a biodegradable polymer blend, reinforced with bio-hydroxyapatite (bio-HAp). First, bio-HAp was obtained from eggshell residues by the wet precipitation method. PLA/PBAT blend with 1.5 wt% of bio-HAp was prepared by melt extrusion and injection molding process. Part of composite samples was irradiated with gamma radiation dose of 25 kGy, at room temperature and presence of air. The effects of the bio-HAp addition into the biodegradable blend were investigated by mechanical tests, XRD, DSC, FESEM, and cytotoxicity “in vitro” analysis and the correlation between the properties was discussed. In addition, the microbiological tests were carried out at irradiated and non-irradiated composite samples in order to evaluate the efficiency of the radiation dose of 25 kGy at composite materials sterilization.

    Palavras-Chave: apatites; polyurethanes; polymers; biodegradation; antimitotic drugs; microorganisms; materials testing

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  • IPEN-DOC 25626

    ROMANO, REBECA da S.G. ; OLIANI, WASHINGTON L. ; KUMAR, VIJAYA R.; PARRA, DUCLERC F. ; LUGAO, ADEMAR B. . Differences in properties of pro-degradant added PP and gamma-irradiated PP under environmental aging. In: LI, BOWEN (Ed.); LI, JIAN (Ed.); IKHMAYIES, SHADIA (Ed.); ZHANG, MINGMING (Ed.); KALAY, YUNUS E. (Ed.); CARPENTER, JOHN S. (Ed.); HWANG, JIANN-YANG (Ed.); MONTEIRO, SERGIO N. (Ed.); BAI, CHENGUANG (Ed.); ESCOBEDO-DIAZ, JUAN P. (Ed.); SPENA, PASQUALE R. (Ed.); GOSWAMI, RAMASIS (Ed.). Characterization of Minerals, Metals, and Materials. Cham, CZ, Switzerland: Springer Nature Switzerland AG, 2019. p. 591-603, (The Minerals, Metals & Materials Series). DOI: 10.1007/978-3-030-05749-7_59

    Abstract: Polypropylene (PP) is used for different sectors of the industry and in consequence produces a large amount of waste discarded at landfills causing serious environmental impacts. Controlled degradation of PP can be achieved by exposing the polymers to defined parameters, such as absorbed radiation dose, weather, oxygen, etc. The aim of this study was to compare two methods of accelerated degradation: gamma irradiation of PP 20 kGy and the incorporation of the commercial pro-degradant d2w® (1 wt%) in PP. Dumbbell samples were manufactured by the injection process and exposed to the environment aging for 90 days. Structural changes in PP macromolecules are created upon exposure to ionizing radiation such as main chain scission, crosslinking and peroxidation (in presence of air). Differential scanning calorimetry (DSC), thermogravimetric analysis (TG), scanning electron microscopy (SEM), energy-dispersive spectroscopy (EDX), X-ray fluorescence, Fourier-transformed infrared spectroscopy (FTIR) and mechanical tests characterized the samples. The samples previously irradiated, PP 20 kGy, after natural aging showed higher oxidation and presence of surface cracks than the PP d2w®. They also showed presence of carbonyl groups and decrease of melting temperature corroborating with oxo-degradation.

    Palavras-Chave: polypropylene; ionizing radiations; gamma radiation; residues; wastes; environment; aging; calorimetry

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  • IPEN-DOC 21507

    SCAGLIUSI, SANDRA R. ; CARDOSO, ELISABETH C.L. ; LUGAO, ADEMAR B. . Effect of gamma radiation on the mechanical and degradation properties of bromobutyl rubber compounds. In: CARPENTER, JOHN S. (Ed.); BAI, CHENGUANG (Ed.); ESCOBEDO, JUAN P. (Ed.); HWANG, JIANN-YANG (Ed.); IKHMAYIES, SHADIA (Ed.); LI, BOWEN (Ed.); LI, JIAN (Ed.); MONTEIRO, SERGIO N. (Ed.); PENG, ZHIWEI (Ed.); ZHANG, MINGMING (Ed.) CHARACTERIZATION OF MINERALS, METALS, AND MATERIALS. 144th . ANNUAL MEETING & EXIBITION, March 15-19, 2015, Orlando, Florida. Proceedings... New York: Wiley , 2015, 2015. p. 1307-1316. DOI: 10.1007/978-3-319-48127-2_156

    Palavras-Chave: gamma radiation; 2-methylpropane; isoprene; rubbers; radiation effects; ionizing radiations; radiolysis; cross-linking

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  • IPEN-DOC 21952

    CAMPOS, REJANE D.; SOTENKO, MARIA; HOSUR, MAHESH; JEELANI, SHAIK; DIAZ, FRANCISCO R.V.; MOURA, ESPERIDIANA A.B.; KIRWAN, KERRY; SEO, EMILIA S.M.. Effect of mercerization and electron-beam irradiation on mechanical properties of high density polyethylene (HDPE)/Brazil nut pod fiber (BNPF) bio-composites. In: CARPENTER, JOHN S. (Ed.); BAI, CHENGUANG (Ed.); ESCOBEDO, JUAN P. (Ed.); HWANG, JIANN-YANG (Ed.); LKHMAYIES, SHADIA (Ed.); LI, BOWEN (Ed.); LI, JIAN (Ed.); MONTEIRO, SERGIO N. (Ed.); PENG, ZHIWEI (Ed.); ZHANG, MINGMING (Ed.) CHARACTERIZATION OF MINERALS, METALS, AND MATERIALS. 144th . ANNUAL MEETING & EXIBITION, March 15-19, 2015, Orlando, Florida. Proceedings... 2015. p. 637-644. DOI: 10.1007/978-3-319-48191-3_80

    Palavras-Chave: composite materials; mechanical properties; brazil; nuts; chemical preparation; irradiation; beams; electrons

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  • IPEN-DOC 25627

    SALES, J.N. ; POVEDA, P.N.S. ; ORTIZ, A. ; VALENZUELA-DIAZ, F.R.; SILVA, L.A. . Effect study of the incorporation of the Green Lake clay in the polypropylene homopolymer properties. In: LI, BOWEN (Ed.); LI, JIAN (Ed.); IKHMAYIES, SHADIA (Ed.); ZHANG, MINGMING (Ed.); KALAY, YUNUS E. (Ed.); CARPENTER, JOHN S. (Ed.); HWANG, JIANN-YANG (Ed.); MONTEIRO, SERGIO N. (Ed.); BAI, CHENGUANG (Ed.); ESCOBEDO-DIAZ, JUAN P. (Ed.); SPENA, PASQUALE R. (Ed.); GOSWAMI, RAMASIS (Ed.). Characterization of Minerals, Metals, and Materials. Cham, CZ, Switzerland: Springer Nature Switzerland AG, 2019. p. 629-636, (The Minerals, Metals & Materials Series). DOI: 10.1007/978-3-030-05749-7_62

    Abstract: The advancement of technology has demanded the development of materials with increasingly lighter and more resistant properties. The development of nanocomposites first started in the mid-80s and contributed for obtaining materials with excellent properties. In this work, Green Lake clay was organophilized and incorporated into a commercial homopolymer polypropylene. The efficiency of organophilization was confirmed by water swelling analysis and, later, by Xray diffraction (XRD) analysis. Composites at 0.5, 1.0 and 2% by weight of clay/polypropylene were prepared by double screw extrusion. The properties of the composite were evaluated by means of Charpy impact resistance, tensile strength at rupture, thermogravimetric analysis (TGA). Crystallinity index was determined by differential scanning calorimetry (DSC). The organophilization processwas efficient, the thermogravimetric analysis showed that there was no decrease in the thermal stability of the composites when compared to pure polypropylene, and the results of the Charpy impact resistance were equivalent when compared to the commercial nucleant composites.

    Palavras-Chave: clays; crystal structure; charpy test; polypropylene; polymers

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  • IPEN-DOC 16354

    OLIANI, WASHINGTON L. ; FERMINO, DANILO M.; LIMA, LUIS F.C.P. de ; LUGAO, ADEMAR B. ; PARRA, DUCLERC F. . Effects of accelerated thermal aging on polypropylene modified by irradiation process. In: CARPENTER, JOHN S. (Ed.); BAI, CHENGUANG (Ed.); ESCOBEDO, JUAN P. (Ed.); HWANG, JIANN-YANG (Ed.); IKHMAYIES, SHADIA (Ed.); LI, BOWEN (Ed.); LI, JIAN (Ed.); MONTEIRO, SERGIO N. (Ed.); PENG, ZHIWEI (Ed.); ZHANG, MINGMING (Ed.) CHARACTERIZATION OF MINERALS, METALS, AND MATERIALS. 144th . ANNUAL MEETING & EXIBITION, March 15-19, 2015, Orlando, Florida. Proceedings... New York: Wiley , 2015, 2015. p. 651-658. DOI: 10.1002/9781119093404.ch82

    Palavras-Chave: aging; polypropylene; thermal degradation; irradiation procedures; decomposition; gamma radiation; cross-linking; morphology

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  • IPEN-DOC 23652

    HARADA, JULIO ; MACEDO, JOSE R.N.; MACHADO, GLAUSON A.F. ; VALENZUELA-DIAZ, FRANCISCO; MOURA, ESPERIDIANA A.B. ; ROSA, DERVAL S.. Effects of carbon black incorporation on morphological, mechanical and thermal properties of biodegradable films. In: IKHMAYIES, SHADIA J. (Ed.); LI, BOWEN (Ed.); CARPENTER, JOHN S. (Ed.); HWANG, JIANN-YANG (Ed.); MONTEIRO, SERGIO N. (Ed.); LI, JIAN (Ed.); FIRRAO, DONATO (Ed.); ZHANG, MINGMING (Ed.); PENG, ZHIWEI (Ed.); ESCOBEDO-DIAZ, JUAN P. (Ed.); BAI, CHENGUANG (Ed.) TMS ANNUAL MEETING & EXHIBITION, 145th; CHARACTERIZATION OF MINERALS, METALS, AND MATERIALS, February 14-18, 2016, Nashville, Tennessee, USA. Proceedings... Hoboken, New Jersey: John Wiley & Sons, Inc., 2016. p. 697-704.

    Abstract: This work evaluates the effects of carbon black incorporation on morphological, mechanical and thermal properties of biodegradable films. The biodegradable composite films based on PBAT/PLA blend and PBAT/PLA blend containing 2 wt. % of carbon black were prepared by me lt extrusion, using a twin screw extruder machine and blown extrusion process. The properties of biodegradable film samples were investigated by tensile tests, XRD, MFI, TGA, DSC and FE-SEM analysis and the correlation between properties was discussed.

    Palavras-Chave: biodegradation; films; carbon black; mechanical properties; composite materials

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  • IPEN-DOC 23651

    GONZALEZ-RUIZ, JESUS; YATACO-LAZARO, LOURDES; VIRGINIO, SUELI ; SILVA-VALENZUELA, MARIA das G. da; MOURA, ESPERIDIANA ; VALENZUELA-DIAZ, FRANCISCO. Effects of graphene oxide addition on mechanical and thermal properties of evoh films. In: IKHMAYIES, SHADIA J. (Ed.); LI, BOWEN (Ed.); CARPENTER, JOHN S. (Ed.); HWANG, JIANN-YANG (Ed.); MONTEIRO, SERGIO N. (Ed.); LI, JIAN (Ed.); FIRRAO, DONATO (Ed.); ZHANG, MINGMING (Ed.); PENG, ZHIWEI (Ed.); ESCOBEDO-DIAZ, JUAN P. (Ed.); BAI, CHENGUANG (Ed.) TMS ANNUAL MEETING & EXHIBITION, 145th; CHARACTERIZATION OF MINERALS, METALS, AND MATERIALS, February 14-18, 2016, Nashville, Tennessee, USA. Proceedings... Hoboken, New Jersey: John Wiley & Sons, Inc., 2016. p. 667-674.

    Abstract: Currently, ethylene vinyl alcohol (EVOH) is one of the oxygen barrier materials most used for food packaging. The addition of graphene oxide nanosheets to the EVOH matrix is employed to improve their mechanical and barrier properties. In this work, films of EVOH- based composites reinforced with graphene oxide were prepared by melt extrusion, using a twin screw extruder machine and blown extrusion process. The graphene oxide was prepared via chemical oxidation of natural graphite and then was exfoliated into nanosheets using the sonochemical method. The composite films samples were characterized using FTIR and DSC analysis. In addition, their mechanical properties were also determined.

    Palavras-Chave: graphene; oxides; composite materials; ethylene; alcohols; films; thermodynamic properties

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  • IPEN-DOC 25628

    MESQUITA, ANDERSON dos S. ; CAVALCANTE, IAN T. ; SILVA, LEONARDO G. de A. e . Electron beam effect on the thermal and mechanical properties analysis of DGEBA/EPDM compound. In: LI, BOWEN (Ed.); LI, JIAN (Ed.); IKHMAYIES, SHADIA (Ed.); ZHANG, MINGMING (Ed.); KALAY, YUNUS E. (Ed.); CARPENTER, JOHN S. (Ed.); HWANG, JIANN-YANG (Ed.); MONTEIRO, SERGIO N. (Ed.); BAI, CHENGUANG (Ed.); ESCOBEDO-DIAZ, JUAN P. (Ed.); SPENA, PASQUALE R. (Ed.); GOSWAMI, RAMASIS (Ed.). Characterization of Minerals, Metals, and Materials. Cham, CZ, Switzerland: Springer Nature Switzerland AG, 2019. p. 637-646, (The Minerals, Metals & Materials Series). DOI: 10.1007/978-3-030-05749-7_63

    Abstract: The aim of this work is to obtain, characterize and irradiate the DGEBA/EPDM compound and compare their thermal and mechanical properties with a non-irradiated DGEBA/EPDM compound. The DGEBA/EPDM compound may be used to cover other materials such as polymers and protect them against high thermal conditions and mechanical effort. The compounds have 0.0, 25.0 and 50.0 wt% of DGEBA. In addition, the compounds were irradiated at 30 and 60 kGy at a dose rate 22.41 kGy/s. The thermal properties (DMA and TGA) and mechanical analysis (tensile strength and elongation at break) were performed. In conclusion, the irradiated DGEBA/EPDM compounds may be used for several applications due to the improvement in their mechanical and thermal properties. Their properties are satisfactory for application that requires stronger material.

    Palavras-Chave: epoxides; ethylene propylene diene polymers; thermodynamic properties; electron beams

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  • IPEN-DOC 23654

    ROMANO, REBECA S.G. ; OLIANI, WASHINGTON L. ; PARRA, DUCLERC F. ; LUGAO, ADEMAR B. . Evaluation of environmental aging of polypropylene irradiated versus pristine. In: IKHMAYIES, SHADIA J. (Ed.); LI, BOWEN (Ed.); CARPENTER, JOHN S. (Ed.); HWANG, JIANN-YANG (Ed.); MONTEIRO, SERGIO N. (Ed.); LI, JIAN (Ed.); FIRRAO, DONATO (Ed.); ZHANG, MINGMING (Ed.); PENG, ZHIWEI (Ed.); ESCOBEDO-DIAZ, JUAN P. (Ed.); BAI, CHENGUANG (Ed.) TMS ANNUAL MEETING & EXHIBITION, 145th; CHARACTERIZATION OF MINERALS, METALS, AND MATERIALS, February 14-18, 2016, Nashville, Tennessee, USA. Proceedings... Hoboken, New Jersey: John Wiley & Sons, Inc., 2016. p. 729-736. DOI: 10.1007/978-3-319-48210-1_92

    Abstract: Polypropylene (PP) is the most common thermoplastic resin of the plastic market due to its very interesting physical, chemical and processing properties at very low market price, however after its use the resin does not degrade in the environment or it degrades at very low rate. This study has the objective of comparing the environmental exposure of PP irradiated with 20 kGy and pristine PP. Dumbbell samples were manufactured by injection molding and exposed to the environment during 90 days; another one set was subjected to gamma irradiation at 20 kGy total dose and exposed at the same conditions too. The samples were characterized by mechanical testing, visual inspection, infrared spectroscopy (IR), scanning electron microscopy (SEM) and differential scanning calorimetry (DSC). The irradiated samples, after environmental aging, showed oxidation and presence of cracks in samples of the PP 20 kGy.

    Palavras-Chave: polypropylene; gamma radiation; environment; aging

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  • IPEN-DOC 22128

    BERENGUER, ISABELLE O. ; OLIANI, WASHINGTON L. ; PARRA, DUCLERC F. ; KOMATSU, LUIZ G.H. ; SANTOS, VINICIUS J. ; LINCOPAN, NILTON; LUGAO, ADEMAR B. ; RANGARI, VIJAYA K.. Fabrication of gamma-irradiated polypropylene and AgNPs nanocomposite films and their antimicrobial activity. In: CARPENTER, JOHN S. (Ed.); BAI, CHENGUANG (Ed.); ESCOBEDO, JUAN P. (Ed.); HWANG, JIANN-YANG (Ed.); IKHMAYIES, SHADIA (Ed.); LI, BOWEN (Ed.); LI, JIAN (Ed.); MONTEIRO, SERGIO N. (Ed.); PENG, ZHIWEI (Ed.); ZHANG, MINGMING (Ed.) CHARACTERIZATION OF MINERALS, METALS, AND MATERIALS. 145th . ANNUAL MEETING & EXIBITION, February 14-18, 2016, Nashville, Tennessee, USA. Proceedings... New York: Wiley , 2016, 2016. p. 143-150. DOI: 10.1002/9781119274896.ch18

    Palavras-Chave: polypropylene; nanocomposites; silver; nanoparticles; silicon

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  • IPEN-DOC 27625

    TATEI, TATIANE Y. ; FONTES, ERIC H. ; MOREIRA, RENAN P. ; DIAS, FRANCISCO V.; OLIVEIRA, RENE R. ; RANGARI, VIJAYA; MOURA, ESPERIDIANA A.B. . Improvement properties of polypropylene by graphene oxide incorporation. In: LI, JIAN (Ed.); ZHANG, MINGMING (Ed.); LI, BOWEN (Ed.); MONTEIRO, SERGIO N. (Ed.); IKHMAYIES, SHADIA (Ed.); KALAY, YUNUS E. (Ed.); HWANG, JIANN-YANG (Ed.); ESCOBEDO-DIAZ, JUAN P. (Ed.); CARPENTER, JOHN S. (Ed.); BROWN, ANDREW D. (Ed.). Characterization of Minerals, Metals, and Materials. Cham, CZ, Switzerland: Springer Nature Switzerland AG, 2020. p. 581-589, (The Minerals, Metals & Materials Series). DOI: 10.1007/978-3-030-36628-5_57

    Abstract: Due to the remarkable properties of graphene oxide (GO) and its possibility of functionalization,GOhas been used in many applications such as nanocomposites. GO nanosheets have been shown to improve the properties of the polypropylene (PP) matrix, for instance, its strength, gas barrier, thermal, and electrical conductivity. As PP has relatively low cost and varied applications, this work aims to study the changes in its thermal, morphological, and mechanical properties, due to the incorporation of GO in the PP matrix. GO was synthesized from graphite by a modified Hummers method. The nanocomposites PP/GO with 0.1, 0.2, and 0.3 wt% of GO in the PP matrix were obtained using a twin-screw extruder and an injection molding machine via a melt blending process. The nanocomposites PP/GO were characterized by FE-SEM and Izod impact test. In addition, the GO nanosheets were also characterized by Raman spectroscopy, ATR-FTIR, FE-SEM, and XRD, therewith correlation between properties was discussed.

    Palavras-Chave: graphene; oxides; polypropylene; nanocomposites

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  • IPEN-DOC 25619

    MARCHINI, LEONARDO G. ; PARRA, DUCLERC F. ; RANGARI, VIJAYA K.. Incorporation of silver nanoparticles in zinc oxide matrix in Polyester Thermoplastic Elastomer (TPE-E) aiming antibacterial activity. In: LI, BOWEN (Ed.); LI, JIAN (Ed.); IKHMAYIES, SHADIA (Ed.); ZHANG, MINGMING (Ed.); KALAY, YUNUS E. (Ed.); CARPENTER, JOHN S. (Ed.); HWANG, JIANN-YANG (Ed.); MONTEIRO, SERGIO N. (Ed.); BAI, CHENGUANG (Ed.); ESCOBEDO-DIAZ, JUAN P. (Ed.); SPENA, PASQUALE R. (Ed.); GOSWAMI, RAMASIS (Ed.). Characterization of Minerals, Metals, and Materials. Cham, CZ, Switzerland: Springer Nature Switzerland AG, 2019. p. 79-88, (The Minerals, Metals & Materials Series). DOI: 10.1007/978-3-030-05749-7_9

    Abstract: The purpose of present study is to evaluate the antimicrobial potential of Thermoplastic Polyester Elastomer (TPE-E) incorporated with zinc oxide added with colloidal dispersion of metallic silver adsorbed on pyrogenic silica (AgNPs_ZnO). A combination of single screw extruder and hot press technique was used to fabricate these polymer nanocomposite films. These polymer nanocomposite films were prepared by mechanical mixing of 1% (w/w) of oil, anti-oxidant 0.05% (w/w), TPE-E granules 0.5% (w/w) and followed by single screw extruder to produce the pellets. As-prepared pellets were further melted for films in hot press technique. Antimicrobial activity was evaluated according to Japan Industrial Standard—JIS Z 2801 in TPE-E compounds against Staphylococcus aureus (S. aureus) and Escherichia coli (E. coli). TPE-E samples containing additives 0.05 and 0.5% AgNPs_ZnO presented 75 and93%bactericidal reduction for Gram-negative bacteria Escherichia coli (E. coli) and 76 and 92% bactericidal activity reduction for Gram-positive bacteria Staphylococcus aureus (S. aureus), respectively.

    Palavras-Chave: silver; nanoparticles; antimicrobial agents; thermoplastics; polyesters; elastomers; zinc oxides

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  • IPEN-DOC 20811

    MACHADO, MESSIAS dos S.; GODOY, RENATO B. ; SILVA, ANDRESSA ; LIMA, ROBERTA; OLIVEIRA, RENE R.; VALENZUELA-DIAZ, FRANCISCO; MOURA, ESPERIDIANA . influence of clay exfoliation on the properties of evoh/clay flexible fims. In: CARPENTER, JOHN S. (Ed.); BAI, CHENGUANG (Ed.); ESCOBEDO, JUAN P. (Ed.); HWANG, JIANN-YANG (Ed.); LKHMAYIES, SHADIA (Ed.); LI, BOWEN (Ed.); LI, JIAN (Ed.); MONTEIRO, SERGIO N. (Ed.); PENG, ZHIWEI (Ed.); ZHANG, MINGMING (Ed.) CHARACTERIZATION OF MINERALS, METALS, AND MATERIALS. 144th . ANNUAL MEETING & EXIBITION, March 15-19, 2015, Orlando, Florida. Proceedings... New York: Wiley , 2015, 2015. p. 273-279. DOI: 10.1002/9781119093404.ch34

    Palavras-Chave: copolymers; ethylene; vinyl acetate; alcohols; clays; films; flexibility; tensile properties; x-ray diffraction; calorimetry

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  • IPEN-DOC 24664

    SANTANA, JULYANA ; SEIXAS, MARCUS V. de S. ; RANGARI, VIJAY; VALENZUELA-DIAZ, FRANCISCO; WIEBECK, HELIO; MOURA, ESPERIDIANA . Influence of electron-beam irradiation on the properties of LDPE/EDPM blend foams. In: LI, BOWEN (Ed.); LI, JIAN (Ed.); IKHMAYIES, SHADIA (Ed.); ZHANG, MINGMING (Ed.); KALAY, YUNUS E. (Ed.); CARPENTER, JOHN S. (Ed.); HWANG, JIANN-YANG (Ed.); MONTEIRO, SERGIO N. (Ed.); FIRRAO, DONATO (Ed.); BROWN, ANDREW (Ed.); BAI, CHENGUANG (Ed.); PENG, ZHIWEI (Ed.); ESCOBEDO-DIAZ, JUAN P. (Ed.); GOSWAMI, RAMASIS (Ed.); KIM, JEONGGUK (Ed.). Characterization of Minerals, Metals, and Materials. TMS. Cham, CZ, Switzerland: Springer International Publishing AG, 2018. p. 547-555, (The Minerals, Metals & Materials Series). DOI: 10.1007/978-3-319-72484-3_58

    Abstract: Closed-cell polyethylene (PE) foams have been extensively used in many applications such as packaging, transportation, sports, construction, and agriculture because of their variety of properties including light weight, chemical resistance, thermal and electrical insulation. The objective of this study is to evaluate the influence of electron-beam irradiation on the properties of LDPE/EPDM blend foams. The LDPE/EPDM blend (80/20 wt%) were prepared by melt extrusion, using a twin-screw extruder machine. The foam structure of LDPE/EPDM blends was obtained by melt extrusion process, using a special single screw for foaming with 1.5 wt% of foaming agent as blowing agent. The foam samples were irradiated by electron-beam at radiation dose of 25, 50, 75 and 100 kGy and submitted to heating in an oven at 100 °C. The specimen tests samples of irradiated and non-irradiated foams were submitted to mechanical tests, DSC, TG analysis and density measurement.

    Palavras-Chave: polyethylenes; ethylene propylene diene polymers; density; irradiation; tensile properties

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  • IPEN-DOC 20812

    SALES, JORGE N. ; SILVA, ANDRESSA A. ; VALENZUELA-DIAZ, FRANCISCO R.; MOURA, ESPERIDIANA A.B. . Influence of the nanoclay cloisite 20A incorporation on properties of acrylonitrile butadiene styrene (ABS). In: CARPENTER, JOHN S. (Ed.); BAI, CHENGUANG (Ed.); ESCOBEDO, JUAN P. (Ed.); HWANG, JIANN-YANG (Ed.); LKHMAYIES, SHADIA (Ed.); LI, BOWEN (Ed.); LI, JIAN (Ed.); MONTEIRO, SERGIO N. (Ed.); PENG, ZHIWEI (Ed.); ZHANG, MINGMING (Ed.) CHARACTERIZATION OF MINERALS, METALS, AND MATERIALS. 144th . ANNUAL MEETING & EXIBITION, March 15-19, 2015, Orlando, Florida. Proceedings... New York: Wiley , 2015, 2015. p. 159-163. DOI: 10.1007/978-3-319-48191-3_20

    Palavras-Chave: acrylonitrile; butadiene; styrene; nanostructures; composite materials; clays; tensile properties

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  • IPEN-DOC 27626

    SANTOS, BIANCA S. ; INACIO, ANDRE L.N. ; BARTOLOMEI, SUELLEN S. ; SILVA, TAISE B.S. ; CARMO, KARINA L.S. ; OLIVEIRA, RENE R. ; MOURA, ESPERIDIANA A.B. . Influence of the reduced graphene oxide incorporation on properties of acrylonitrile butadiene styrene (ABS). In: LI, JIAN (Ed.); ZHANG, MINGMING (Ed.); LI, BOWEN (Ed.); MONTEIRO, SERGIO N. (Ed.); IKHMAYIES, SHADIA (Ed.); KALAY, YUNUS E. (Ed.); HWANG, JIANN-YANG (Ed.); ESCOBEDO-DIAZ, JUAN P. (Ed.); CARPENTER, JOHN S. (Ed.); BROWN, ANDREW D. (Ed.). Characterization of Minerals, Metals, and Materials. Cham, CZ, Switzerland: Springer Nature Switzerland AG, 2020. p. 599-607, (The Minerals, Metals & Materials Series). DOI: 10.1007/978-3-030-36628-5_59

    Abstract: The purpose of this study was to evaluate the influence of incorporation of the reduced graphene oxide on properties of acrylonitrile butadiene styrene (ABS). The incorporation of 0.5 and 1.5 wt% of RGO into ABS matrix was carried out by melting extrusion process using a twin-screw extruder and injection molding machine. The properties of ABS/RGO nanocomposite samples were investigated by tensile and impact Izod tests, FE-SEM, and XRD analysis. The results showed that the incorporation of small amount of RGO into ABS matrix led to obtaining of polymeric nanocomposite with superior mechanical properties when compared with original properties of ABS matrix.

    Palavras-Chave: graphene; oxides; acrylonitrile; butadiene; styrene; mechanical tests

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A pesquisa no RD utiliza os recursos de busca da maioria das bases de dados. No entanto algumas dicas podem auxiliar para obter um resultado mais pertinente.

✔ É possível efetuar a busca de um autor ou um termo em todo o RD, por meio do Buscar no Repositório , isto é, o termo solicitado será localizado em qualquer campo do RD. No entanto esse tipo de pesquisa não é recomendada a não ser que se deseje um resultado amplo e generalizado.

✔ A pesquisa apresentará melhor resultado selecionando um dos filtros disponíveis em Navegar

✔ Os filtros disponíveis em Navegar tais como: Coleções, Ano de publicação, Títulos, Assuntos, Autores, Revista, Tipo de publicação são autoexplicativos. O filtro, Autores IPEN apresenta uma relação com os autores vinculados ao IPEN; o ID Autor IPEN diz respeito ao número único de identificação de cada autor constante no RD e sob o qual estão agrupados todos os seus trabalhos independente das variáveis do seu nome; Tipo de acesso diz respeito à acessibilidade do documento, isto é , sujeito as leis de direitos autorais, ID RT apresenta a relação dos relatórios técnicos, restritos para consulta das comunidades indicadas.

A opção Busca avançada utiliza os conectores da lógica boleana, é o melhor recurso para combinar chaves de busca e obter documentos relevantes à sua pesquisa, utilize os filtros apresentados na caixa de seleção para refinar o resultado de busca. Pode-se adicionar vários filtros a uma mesma busca.

Exemplo:

Buscar os artigos apresentados em um evento internacional de 2015, sobre loss of coolant, do autor Maprelian.

Autor: Maprelian

Título: loss of coolant

Tipo de publicação: Texto completo de evento

Ano de publicação: 2015

✔ Para indexação dos documentos é utilizado o Thesaurus do INIS, especializado na área nuclear e utilizado em todos os países membros da International Atomic Energy Agency – IAEA , por esse motivo, utilize os termos de busca de assunto em inglês; isto não exclui a busca livre por palavras, apenas o resultado pode não ser tão relevante ou pertinente.

✔ 95% do RD apresenta o texto completo do documento com livre acesso, para aqueles que apresentam o significa que e o documento está sujeito as leis de direitos autorais, solicita-se nesses casos contatar a Biblioteca do IPEN, bibl@ipen.br .

✔ Ao efetuar a busca por um autor o RD apresentará uma relação de todos os trabalhos depositados no RD. No lado direito da tela são apresentados os coautores com o número de trabalhos produzidos em conjunto bem como os assuntos abordados e os respectivos anos de publicação agrupados.

✔ O RD disponibiliza um quadro estatístico de produtividade, onde é possível visualizar o número dos trabalhos agrupados por tipo de coleção, a medida que estão sendo depositados no RD.

✔ Na página inicial nas referências são sinalizados todos os autores IPEN, ao clicar nesse símbolo será aberta uma nova página correspondente à aquele autor – trata-se da página do pesquisador.

✔ Na página do pesquisador, é possível verificar, as variações do nome, a relação de todos os trabalhos com texto completo bem como um quadro resumo numérico; há links para o Currículo Lattes e o Google Acadêmico ( quando esse for informado).

ATENÇÃO!

ESTE TEXTO "AJUDA" ESTÁ SUJEITO A ATUALIZAÇÕES CONSTANTES, A MEDIDA QUE NOVAS FUNCIONALIDADES E RECURSOS DE BUSCA FOREM SENDO DESENVOLVIDOS PELAS EQUIPES DA BIBLIOTECA E DA INFORMÁTICA.

O gerenciamento do Repositório está a cargo da Biblioteca do IPEN. Constam neste RI, até o presente momento 20.950 itens que tanto podem ser artigos de periódicos ou de eventos nacionais e internacionais, dissertações e teses, livros, capítulo de livros e relatórios técnicos. Para participar do RI-IPEN é necessário que pelo menos um dos autores tenha vínculo acadêmico ou funcional com o Instituto. Nesta primeira etapa de funcionamento do RI, a coleta das publicações é realizada periodicamente pela equipe da Biblioteca do IPEN, extraindo os dados das bases internacionais tais como a Web of Science, Scopus, INIS, SciElo além de verificar o Currículo Lattes. O RI-IPEN apresenta também um aspecto inovador no seu funcionamento. Por meio de metadados específicos ele está vinculado ao sistema de gerenciamento das atividades do Plano Diretor anual do IPEN (SIGEPI). Com o objetivo de fornecer dados numéricos para a elaboração dos indicadores da Produção Cientifica Institucional, disponibiliza uma tabela estatística registrando em tempo real a inserção de novos itens. Foi criado um metadado que contém um número único para cada integrante da comunidade científica do IPEN. Esse metadado se transformou em um filtro que ao ser acionado apresenta todos os trabalhos de um determinado autor independente das variáveis na forma de citação do seu nome.

A elaboração do projeto do RI do IPEN foi iniciado em novembro de 2013, colocado em operação interna em julho de 2014 e disponibilizado na Internet em junho de 2015. Utiliza o software livre Dspace, desenvolvido pelo Massachusetts Institute of Technology (MIT). Para descrição dos metadados adota o padrão Dublin Core. É compatível com o Protocolo de Arquivos Abertos (OAI) permitindo interoperabilidade com repositórios de âmbito nacional e internacional.

1. Portaria IPEN-CNEN/SP nº 387, que estabeleceu os princípios que nortearam a criação do RDI, clique aqui.


2. A experiência do Instituto de Pesquisas Energéticas e Nucleares (IPEN-CNEN/SP) na criação de um Repositório Digital Institucional – RDI, clique aqui.

O Repositório Digital do IPEN é um equipamento institucional de acesso aberto, criado com o objetivo de reunir, preservar, disponibilizar e conferir maior visibilidade à Produção Científica publicada pelo Instituto, desde sua criação em 1956.

Operando, inicialmente como uma base de dados referencial o Repositório foi disponibilizado na atual plataforma, em junho de 2015. No Repositório está disponível o acesso ao conteúdo digital de artigos de periódicos, eventos, nacionais e internacionais, livros, capítulos, dissertações, teses e relatórios técnicos.

A elaboração do projeto do RI do IPEN foi iniciado em novembro de 2013, colocado em operação interna em julho de 2014 e disponibilizado na Internet em junho de 2015. Utiliza o software livre Dspace, desenvolvido pelo Massachusetts Institute of Technology (MIT). Para descrição dos metadados adota o padrão Dublin Core. É compatível com o Protocolo de Arquivos Abertos (OAI) permitindo interoperabilidade com repositórios de âmbito nacional e internacional.

O gerenciamento do Repositório está a cargo da Biblioteca do IPEN. Constam neste RI, até o presente momento 20.950 itens que tanto podem ser artigos de periódicos ou de eventos nacionais e internacionais, dissertações e teses, livros, capítulo de livros e relatórios técnicos. Para participar do RI-IPEN é necessário que pelo menos um dos autores tenha vínculo acadêmico ou funcional com o Instituto. Nesta primeira etapa de funcionamento do RI, a coleta das publicações é realizada periodicamente pela equipe da Biblioteca do IPEN, extraindo os dados das bases internacionais tais como a Web of Science, Scopus, INIS, SciElo além de verificar o Currículo Lattes. O RI-IPEN apresenta também um aspecto inovador no seu funcionamento. Por meio de metadados específicos ele está vinculado ao sistema de gerenciamento das atividades do Plano Diretor anual do IPEN (SIGEPI). Com o objetivo de fornecer dados numéricos para a elaboração dos indicadores da Produção Cientifica Institucional, disponibiliza uma tabela estatística registrando em tempo real a inserção de novos itens. Foi criado um metadado que contém um número único para cada integrante da comunidade científica do IPEN. Esse metadado se transformou em um filtro que ao ser acionado apresenta todos os trabalhos de um determinado autor independente das variáveis na forma de citação do seu nome.